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Structures and Materials Division Research and Technology Directorate NASA Glenn Research Center

Analytical Science Group
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Analytical Chemistry
Electron Optics
Metallography
Optical Lab
Sample Preparation
XRay Diffraction
Gallery
Metallography Lab
Sample Preparation: Polishing
Polishing techniques used to prepare general samples involve four major steps: Plane Grind, Fine Grind, Diamond Polishing and Vibratory Polishing. For more unique samples a special set of polishing steps will be developed to fit the needs of the sample.

Variety of prepared samples
 
Above: Polishing operations in the Met Lab.
 

Polishing Techniques
Plane Grind
  • Rough grind of sample to produce a flat surface
  • Step removes any excess epoxy or hardened Bakelite powder that may have covered the sample surface
Fine Grind
  • Series of fine grinding steps which ultimately produce a 20 micron finish
Diamond Polishing
  • Produces a 1 micron finish
  • Several rotating disks are used in the process each time reducing the size of the scratches
Vibratory Polishing
  • Refines surface using 0.5 micron diamond or 0.05 micron colloidal silica.
Return to sample preparation page...
Examples
For further information please contact Joy Buehler
Capabilities
Mounted samples in the Met Lab
Cutting
Mounting samples in the Met Lab
Mounting
Plasma etched sample in the Met Lab
Plasma Etching
Ceramic composite after intereference layering
Interference Layering


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Last Updated: May 13, 2008